By Stanley R. Sandler and Wolf Karo (Auth.)
This revised and up-to-date moment version of Polymer Synthesis II maintains within the culture of quantity I in providing designated laboratory directions for the guidance of varied polymers. every one bankruptcy is equipped via practical teams, and every bankruptcy not just provides preparative equipment, but in addition features a short introductory precis, experiences of the very most modern magazine articles and patents, and protection dangers and precautions. methods were selected at the foundation of protection issues and straightforwardness of being performed with ordinary laboratory gear. This accomplished therapy of every polymer crew makes Polymer Synthesis II an quintessential advisor for business and educational chemists in addition to for college students within the box.
Key Features
* This revised edition:
* Covers every one polymer type, seriously referencing those with patent literature to demonstrate advertisement applications
* presents new and up to date info for every sensible crew, including:
* Curing brokers for epoxy resins
* Polymerization of vinyl ethers and copolymers
* Polyvinyl silfides
* Polymerization of vinyl pyrrolidone and copolymers
* good points multiplied information tables and up to date references
* provides a variety of citations to new catalysts for every polymer education regarding ureas
* features a new section--Complex Formulation--involving the instruction of polyacrylic acid and its copolymers
* comprises many new arrangements, including:
* instruction of t-butyl acrylate copolymers utilizing the Teyssie Method
* Template polymerization of vinylimidazole on polymethacrylic acid
* Polymerization of aqueous acrylic acid utilizing AIBN
* instruction of polyketals by means of transketalization
* Copolymerization of maleic anhydride with ethyl vinyl ether
* complicated and template polymerizations
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Example text
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Mol. wt. = 230). For details, see L. Boldizar, Macromol. Synth. 3, 49 (1969). d This reaction can also be carried out at r o o m temperature over a twoweek period to give a quantitative yield, m . p . 150°-154°C. 30 (w) (where s = strong, m = medium and w = weak). 3-3. H Preparation of Trimethylolmelamine Various Conditions [57] 2 N V N V N H N^Î NH HOCH HN\^N\^NHCH OH 2 2 + 3CH =0 2 2 under • 2 J Î (30) 3. 5 TV sodium hydroxide was added. The temperature fell, and when it was restored to 60°C within 4 min the para formaldehyde dissolved almost completely.