By Petr Zuman, R. Belcher and L. Gordon (Auth.)
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Collect. Czechoslov. Chem. Commun. 25, 3025 (1960). (44) BERG, H. ,Jf. Electroanalyt. Chem. 1, 108 (1959/60). , Z. Elektrochem. 64,1104 (1960); Naturwiss. 47, 320 (1960); 48, 100 (1961). (46) BREZINA, M. , Polarography in Medicine, Biochemistry and Pharmacy, Interscience, New York (1958), where the literature is extensively quoted. 31 INTRODUCTION (47) ZUMAN, P. and Κυικ, Μ . , Collect. Czechoslov. 3861 (1959). Chem. Commun. 2 4 , (48) V O N STACKELBERG, M . a n d FASSBENDER, H . , Z. Elektrochem.
Close both taps A and B during this treatment. Place the solution to be analysed into the left compartment, ensuring that tap B and the stopcock at the bottom of this compartment are closed. Then place the capillary (in a rubber bung) into the solution and allow the mercury to flow out. Introduce the inert gas through the side POLAROGRAPHIC INSTRUMENTATION 39 tube into the solution (Fig. 20d, extreme left) and connect the gas-outlet, the side arm at the top of the left compartment, to a water seal.
5, 148 (1933). , Z. Elektrochem. 48, 278 (1942). , Z. Elektrochem. 49, 164 (1943); Chem. listy 41, 8 (1947). (7) BRDICKA, R. , Naturwiss. 31, 247 (1943); Collect. Czechoslov. Chem. Commun. 12, 39 (1947); 12, 138 (1947). , Collect. Czechoslov. Chem. Commun. 12, 212 (1947). (9) BRDICKA, R. , J. Amer. Chem. Soc. 76, 907 (1954). (10) KOUTECKY, J. , Collect. Czechoslov. Chem. Commun. 12, 337 (1947). , HANUS, V. , General Theoretical Treatment of the Polarographic Kinetic Currents, in Progress in Polarography (P.