By Jessica Ress
All-natural good looks product recipes for fit, sparkling epidermis and a happier you!
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Read or Download 100 Organic Skincare Recipes: Make Your Own Fresh and Fabulous Organic Beauty Products PDF
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Extra resources for 100 Organic Skincare Recipes: Make Your Own Fresh and Fabulous Organic Beauty Products
Sample text
Therefore, in the case of complexes with monodentate phosphines, the initially formed cis-[PdRXL2] (5) complexes undergo isomerization to form the more stable trans-[PdRXL2] complexes [80]. Such isomerization is obviously not possible for complexes 6 with cis-coordinating bidentate phosphines. 5). The isomerization of cis-7 to trans-8 is a rather complex process that can take place by four major competitive pathways. Two of these pathways involve associative replacements of PPh3 by an iodide ligand of a second palladium complex.
The observed configuration is a consequence of the oxidative addition step. This reaction proceeds with complete or predominant retention in noncoordinating solvents [66, 67], which is in agreement with theoretical studies on the oxidative addition of CH3 X to Pd(0) [68]. On the other hand, in coordinating solvents such as MeCN or DMSO, complete or nearly complete inversion was observed [66]. Syn oxidative addition has also been observed in related substrates [69]. However, the usual inversion of configuration in the oxidative addition was observed with [Pd(PPh3 )4 ] [66, 70].
Intramolecular oxidative additions of C–C bonds to Pt(II) to form hexacoordinated Pt(IV) complexes is also known [203]. 20). The oxidative addition occurs intramolecularly on a palladacycle 22 with a particularly electron-rich Pd(II) center to form 24 via intermediate 23. Although Pd(IV) complexes related to 24 can undergo insertion reactions with styrene and alkyl acrylates in a Heck process, the catalytic cycle involved is probably not particularly pertinent to most Heck catalytic Heck reactions [204b].